Building the phosphate and lubricant chain for fastener wire
8 min read
Cold heading is a different lubrication problem from wire drawing: surface area multiplies in a single blow and fresh, unlubricated metal appears underneath. The carrier layer has to keep up with that expansion.
The head of a bolt is formed in a single blow of the press. In that blow the material flows, the surface area in the head region multiplies several times over, and underneath that new surface fresh metal appears — metal that has never met a lubricant. In wire drawing the lubrication problem concerns a continuous surface passing through a die. In cold heading the problem concerns a surface that comes into existence and has to be lubricated in the same instant. That difference explains why surface preparation on a fastener line has to be managed more tightly than on a drawing line.
This article covers the preparation of wire used to make bolts, nuts and similar fasteners: where cold heading departs from wire drawing, what is expected of the zinc phosphate coating in this application, how lubricant selection changes, and the mistakes seen most often on the shop floor. For the general mechanism of friction, see friction in cold forming; for a comparison of the lubricant families, see wire drawing lubricant selection.
Why cold heading is harder than wire drawing
Both are cold forming and both use the same chemical chain, but what is asked of the lubricant is not the same. The differences come down to this:
Surface expansion: In wire drawing the surface area grows by a comparatively limited ratio and the growth is gradual along the die. In cold heading the surface area multiplies at a single station as the head forms.
Fresh metal exposure: Under the expanding surface comes new metal carrying neither phosphate layer nor lubricant. The carrier layer has to stretch with it.
Contact pressure: Contact pressure in a heading die is markedly higher than in a drawing die and is concentrated at one point.
Direction of deformation: In drawing the material mainly elongates along the axis; in heading it flows radially and is pressed against the die face.
Multi-station production: A fastener press forms in several successive stations; the film has to survive from the first to the last.
The practical consequence is that in cold heading the lubricant cannot be judged on its own. Its performance is inseparable from how the phosphate layer beneath it behaves under deformation.
Surface expansion: the real problem in cold heading
A zinc phosphate layer is crystalline and porous, and it is chemically bonded to the metal — it is not a paint applied on top. That bond lets the layer deform together with the material. As the surface expands during head formation the crystal structure opens with it, the pores spread apart, and the lubricant held inside them is distributed across the new area. That is how the system works: the layer does not merely carry the lubricant, it distributes it at the moment of deformation.
This mechanism breaks down at both extremes. When coating weight is too low the layer cannot keep up with the expansion, bare metal is left in the opened region, and it contacts the die directly — galling begins. When the coating is heavier than needed and the crystal structure is coarse, the layer fractures rather than holding under deformation and produces debris; the fragments build up on the die face and mark the product. The right point lies between these extremes and shifts with the degree of deformation.
The steps of the chain
In fastener production the preparation from wire rod to press typically follows this sequence:
Descaling: The oxide layer carried over from hot rolling is removed mechanically or by acid. If scale remains, the phosphate layer sits on the oxide rather than on the surface beneath it.
Degreasing: Rolling residues, protective oils and dust are removed in an alkaline or neutral bath.
Rinsing: Cascade rinsing keeps bath residues from being carried forward.
Activation: Crystal nucleation is set here; a fine and uniform crystal structure is decided at this step.
Neutralising and lubricant: The surface is neutralised, then the lubricant is applied.
Drying and cold heading: The wire goes to the press.
The most frequently skipped link in the chain is the first one. When scale is not fully removed from the wire rod, the result is defective even if every following step works correctly: the phosphate layer sits on the oxide, lifts away with it at the first deformation, and bare metal is exposed underneath. This is usually reported as "the coating isn't holding" — but the problem is not in the coating, it is in the surface itself. For how the activation step governs crystal size, see the activation bath and crystal size.
What the phosphate layer must deliver on fastener wire
The same bath serves both applications, but the weighting of what is expected from the layer shifts. The table below compares the two.
Criterion
Wire drawing
Cold heading (fasteners)
Dominant load
Continuous friction along the die
High contact pressure at a single station
Change in surface area
Gradual and limited
Sudden and large; multiplies in the head region
Crystal structure requirement
Porosity to hold the lubricant
Porosity plus the ability to stretch with deformation
Coating weight decision
Driven by the reduction schedule
Driven by degree of deformation; thickness alone is not enough
Dominant failure mode
Film thinning, die wear, surface scoring
Galling, material pick-up on the die, cracking at the head
What the lubricant must do
Hold film continuity from die to die
Spread without gaps during sudden expansion
Effect of the next step
Residue management if welding, galvanising or heat treatment follows
Residue is usually critical before plating or heat treatment
What the carrier layer must deliver: wire drawing vs cold heading
The most important row is the second from last. In drawing, film continuity decides the outcome; in heading, spreading behaviour does. If two lines running the same coating weight produce cleanly on one and gall on the other, the first place to look is not thickness but the fineness and uniformity of the crystal structure.
The lubricant side: what changes the choice
Dry lubricants divide into reactive families, which react with the phosphate layer, and neutral families, which leave only a physical film. The detailed comparison is in wire drawing lubricant selection; here we take only the part specific to cold heading.
Three inputs decide the choice in heading. The first is the degree of deformation: as head volume grows and the number of stations rises, so does the durability asked of the film. The second is material grade; as alloy content rises, both the formation of the phosphate layer and the behaviour of the lubricant change. The third, and usually the last to be noticed, is what the part will see after heading. Fasteners are largely plated or heat treated, and lubricant and phosphate residue left on the surface can spoil plating adhesion or contaminate a furnace atmosphere at those steps. For removal methods, the approaches in removing drawing soap and phosphate residue apply.
Five mistakes seen most often
Incomplete descaling: The phosphate layer sits on the oxide and lifts away with it at the first deformation. The report says the coating isn't holding; the coating is not the problem.
Treating coating weight as the only target: With g/m² in the right range but a coarse crystal structure, the layer fractures under deformation and produces debris.
Not tracking bath acid balance: When the ratio of total to free acid drifts, the crystal structure changes with it; for method and intervals see phosphate bath maintenance.
Assuming the lubricant will rescue the coating: Putting more lubricant on an inadequate or damaged carrier layer hides the symptom briefly without removing its cause.
Ignoring intermediate storage: Phosphated wire held in a damp environment can start to rust; for conditions and durations see storing phosphated wire.
A checklist for your line
Clarifying these points before requesting a sample or a quote noticeably reduces the number of trials:
Product and deformation: Which fastener is produced, what is the head volume and the number of stations?
Material: Carbon or low-alloy steel; what is the wire rod diameter and grade?
Incoming wire rod: Is scale removed mechanically or by acid, and is the incoming surface checked?
Phosphate line: What are the bath temperature, process time and the measured coating weight range?
Bath control: How often are total and free acid titrated, and are the results recorded?
Lubricant: Which type is used, how is it applied and what are the drying conditions?
After heading: Is there plating, heat treatment or surface cleaning, and what is the residue acceptance criterion?
Intermediate stock: How long and under what conditions does phosphated wire wait?
Once these are filled in, whether the problem comes from the carrier layer or from the lubricant usually separates out at the first assessment. For technical data sheets see the document center, and to determine the right KIMSOL and Kimkal combination for your press layout, get in touch.
Frequently asked questions
Why is lubrication harder in cold heading than in wire drawing?
In wire drawing the surface area grows gradually and by a limited ratio along the die. In cold heading the surface area multiplies at a single station as the head forms, and fresh metal carrying no lubricant at all appears under the expanding surface. The phosphate carrier layer has to stretch along with that expansion and distribute the lubricant over the new surface.
What coating weight should be used for fastener wire?
There is no single correct value. KIMSOL baths are run in the 3–15 g/m² range; where within that range a line should sit is set by the part's degree of deformation, the material grade and the press layout. Thickness on its own is not a sufficient target — the fineness and uniformity of the crystal structure matter at least as much as coating weight.
If galling appears on the heading die, where should you look first?
Before changing the lubricant, verify in order whether scale was fully removed from the wire rod surface, what the coating weight is, and whether the balance of total and free acid in the bath is under control. Galling usually comes not from an inadequate lubricant but from a carrier layer that tears or fractures under deformation.
Does phosphate and lubricant residue after heading cause problems?
Fasteners are largely plated or heat treated. Residue left on the surface before those steps can spoil plating adhesion or contaminate the atmosphere in a controlled-atmosphere furnace. For that reason lubricant selection should account not only for heading performance but also for how and at which step the residue will be removed.
In fastener production the surface expands several-fold; a liquid oil cannot carry that contact pressure. We explain how the porous phosphate layer and the soap film work together, and how the pair is selected by severity of deformation.
Reactive soap reacts with the phosphate layer to form zinc soap; neutral soap leaves a physical film. Which suits which line is decided by drawing speed, reduction ratio, wire diameter and what the wire has to go through after drawing.
Phosphate coating is not a single tank but a connected chain: degreasing, rinsing, activation, phosphating, soap and drawing. This guide summarises each stage end to end — what it does, its typical parameters and how it affects the next one.